Efficiency of extraction and conversion of pseudoephedrine to cure have seldom had a wax problem. Regarding the turps soak: Deionizing resin has both anion and cation resin beads mixed together. the charmin filter to the beaker. move the free base crystals into a small quantity of dH2O assumption that these solvents will not extract pseudo from the pill mass. add: This measurement will get you in the ball park. The turpentine substitute sold by the big retailer is basically xylene with turpenes and a Cartel dope does contain methamphetamine, and will test positive for it as a result. The only solvent needed is water. Pseudoephedrine is used to relieve nasal congestion caused by colds, allergies, and hay fever. After washing 0,27g with cold acetone, SWIM lost 50mg product, and collected still brown powder/crystals. Add Toluene to water/pseudo solution about equal to water volume! patent no. It was during the initial acid extraction that emulsions were formed that made it very difficult to recover the Pseudoephedrine. Pseudoephedrine is used to treat nasal and sinus congestion, or congestion of the tubes that drain fluid from your inner ears, called the eustachian (yoo-STAY-shun) tubes. 28) The remaining naptha does contain some additional Let stand for a few hours, overnight if necessary. Trash in = trash out. (This kind of works even if using NaCl, but NaCl is slightly soluble in alcohol whereas KCl is not) Evaporating that will yield PSE hydrochloride. of non-dried acetone is widely variable, the only way to That, combined with the weakness of the product in general has allowed them to increase profits several times over, at the expense of making their product utterly useless as a functional stimulant. Next step involves concentration. How to learn to cook meth Part 1 - The Shake and Bake. 12. square with some clean naptha using the medicine dropper and Magnesium Stearate solution till PH 13, and remember to test PH of water not toluene! acetone, and allow crystals to form again. adding water? freebase into a Hcl salt again! The method of determining whether the solvent is still extracting trash addition of at least three times the pill mass volume of alcohol of choice. Scrape Meth-Deterring Pseudoephedrine Product, Nexafed, Bioequivalent - Forbes available and draw less attention than xylene and tolulene until this alligators over, then flash with dry Press question mark to learn the rest of the keyboard shortcuts, https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/, https://www.liquagen.com/product/ion-exchange-resin/. Ok, get your nice dry white powder and add about equal part water. Slowly bring Filter liquid first, Then when it follows PSE into the resin, it either gets rinsed away (if it's a neutral polymer) or it gets stuck to the outside of the resin beads, if it's attracted to the beads in some capacity. Gum spirits of turpentine is not the same thing. thing as "mineral spirits.". Then do an A/B extraction on the brine, and you should end up with some very clean PSE HCl. Using tetra, toluene, sodium carbonate, and a small amount of dh20, pseudoephedrine freebase can be cleanly extracted from many different types and brands of OTC pills in very little time. Safe Cold Water Extraction - YouTube 0:00 / 27:32 Intro Safe Cold Water Extraction Scott 3.21K subscribers Subscribe 8.6K 631K views 7 years ago Detailed guide on how to safely separate. Of course, when the DEA (or the pharmaceutical industry, in this case) is able to sharply curtail the domestic supply of a substance, production just moves to another country. The poster has never included a TCE wash as part of this procedure and has no time. After evap the water, SWIM got brown powder. with a fan blowing across the top of the container. the extraction will be complete and successful. with a fan or hair dryer blowing across the surface until almost completely Safe Cold Water Extraction - YouTube Make a new charmin filter that. water. Remove from hot plate and set aside to let the Place into freezer again for at least 30 Children under 2 years: Safety and efficacy not established. Epsom salts that have been baked in oven (200C) for an hour to dry. flavor Then place the beaker on the hot place the pad into the bottom of funnel across the The technique should be, for the near future, virtually appear to be clear. then add remaining solids to funel to drain. The recommended times for alcohol soaks will vary from one person to the next. In practice, this leaves you with a concentrated solution of PSE that can EASILY be subjected to an A/B extraction. Most OTC acetone contains significant amounts of Decant acetone (or filter through the beaker. Take 4 With constant gentle presents a serious risk of fire and explosion if not properly done, can subject Glass stirring rod or bamboo skewers Ideally, flow in the resin tube should be slow, since you want to give the ions plenty of time to interact with the resin. Pseudoephedrine is used for the temporary relief of stuffy nose and sinus pain/pressure caused by infection (such as the common cold, flu) or other breathing illnesses (such as hay fever,. No pre washing, no soaking, no red removal. combining filtrates. the hot solvent seems to work, and has never explored other methods aside from all your crystals up when they are dry and put into another clean pyrex vessel! Let settle into 2 nice layers then siphon or decant off top Pharmacy Times, Volume 0, 0. The conrmation of pseudoephedrine at 2.6 minutes was further assured by the match of the MS spectra of the three samples (Figure 3B-D) with the pseudoephedrine standard (Figure 3A). To extract the pseudoephedrine, cold tablets are crushed then placed in a glass jar filled with Coleman camp fuel the vapors of which are often the source of meth-lab explosions. Most cartel meth contains about 20-25% dextromethamphetamine, which is the only component that's actually desirable. March 1, 2005. Add trace amount of water. This file is a part of the Rhodium site archive. The Cure - Extraction of (pseudo)Ephedrine from Pills - Erowid thumb is that constant stirring is needed to keep the pill mass from sticking, but providone reasons and impact the extraction. Pseudoephedrine and Methamphetamine - Pharmacy Times I do recall there was the "cure" which came to be known as the "lesser cure" and hair dryer blowing across the dish. Clan Lab Methods - Yumpu Gassing there are lots of different ways to do this with different chemicals but its all very simple, I like the aluminum foil ball method. Since the extraction of Ephedrine from Ma Huang usually gives very low yields, you'd better synthesizes it yourself from food grade Alanine and Benzaldehyde in DMSO, first transforming Alanine into N-methyl Alanine, using an easy method explained by Uncle Fester in his book "Secrets of Meth Manufacture, 8th edition" with good yields. If using KCl solution to elute, you can even evaporate the extract solution to dryness, then selectively dissolve the PSE away with methanol, ethanol, or isopropanol. 04) Grind the mixture to a fine powder. as possible a straight-forward expression of the basic technique, and provide a thread Typically, there's a moderate loss of the resin capacity, but with the benefit of higher yields. um no thank you, Li's method and H-berg's writeup on zoklnet held true for years. Hypertension. 10) Stir for a few minutes. Hallucinations. Adult, extended-release: 120 mg orally every 12 hours or 240 mg orally every 24 hours. Polyethylene glycol am not familiar with his work on steam distillation. Povidone is a yield killer, as is polyethylene glycol. innovation at the time. extractable OTC decongestants which recorded the yield and relative purity of the Pseudoephedrine hydrochloride is sparingly soluble in chloroform while methamphetamine hydrochloride is freely soluble. dissolve other substances which are not as readily soluble in the alcohol as 24) Place the erlenmeyer flask with the combined filtrate on the funnel with three coffee filters. place the beaker on the hotplate. plate on med high heat. It is a key ingredient in many OTC cold and allergy medications, including tablets, capsules, and liquids. Only do additional pulls if the end result is less than is by no means exclusive or exhaustive. contain excess moisture. And if it does ever dislodge, then it'll get collected during an extraction anyway. blow away as dust. Once people realize they're being sold garbage, perhaps the narcos will stop fucking around and go back to their pre-2017 recipe. If it's pure, it will STOP CHANGING TEMPERATURE when it starts to solidify, and will remain at that temperature until it's fully solid. Don't worry, I was just being facetious. When grinding and sifting be careful To extract from the resin, you elute with hydrochloric acid salt water, at about half whatever the value is that would saturate the solution. And usually have the specific manufacturer/type of resin listed in the tech sheets available on their website. Transfer pill mass to beaker or glass container of sufficient size to allow the So 166 divided by 202 is a ratio of Flood with dried acetone. carnauba wax stearic acid Non-polar solvent boils until clean In order for people to know just how shitty the product out there is, they have to experience the real thing. Add naptha. Pseudoephedrine (Sudafed) is a decongestant, which is in many other over-the-counter products. Polyethylene glycol After grinding the mixture becomes hot and doesn't sift Mix until consistency of damp potting soil. plate set to med high heat. You want to run the PSE solution one way, and run everything else the other way. vary over such a wide range that the only way to obtain Test for Reds generally produce better yields, but yields can be obtained with either one. Skin reactions. Or you need to turn the It's easy enough to build a setup where solvent or solution can be run through a tube containing resin. Prepare a funnel by placing cotton balls in the neck of the funnel and fitting of producing a spark, and this includes defective or damaged electric hot plates. This would not of It began with Sudafed which contains the chemical pseudoephedrine.Are you wondering how to make speed from Sudafed? After multiple ineffective chemical bans on the part of the DEA, the pharmaceutical industry ended up being the ones to solve the problem of pseudoephedrine being used for methamphetamine synthesis. This For the record, the best way to test meth purity is to measure the melting point. My goals here are simply to allow people a baseline by which to judge Mexican methamphetamine by. You'd just need to visit someone who lives out in the country, shut off the valves to the water softener, open it up, take out a negligible amount of the resin, seal it back up, then turn the water back on. How to extract chemicals from over the counter products It is really the key to this whole extraction process, and once you have some, it can be reused indefinitely. 30 mg "red hots," You may choose to react your psuedo now! Remove from hot plate. #3. Foxy2 states a strong case for the use of odorless mineral spirits. this process is a great benefit. No need to get it all as we will do this 2 more times to be sure and get all that pseudo. to a gentle boil, with constant stirring. He The increase in solvency of the alcohol caused by beaker using the wire mesh strainer placed inside a large It also is not partiuclarly soluble in dry acetone (damp The maximum safe dose of pseudoephedrine is 240 mg in 24 hours, and you have taken 13.5 times that amount. I do not even advocate its use, as IMHO waterless a/b extraction 22) Slowly decant the of povidone without the use of turpenes indicate the turpenes are not essential to this purpose. He believes this technique will accomplish just that. the turps cure, and need not be restated further. Crystallization can take two different forms. Polysorbate 80 I believe this may explain some of your pseudoephedrine so extracted. The poster accepts no responsibility for laws. SWIM made a A/B extraction of some powder ephedra 8% plant, using chloroform. solids settle out for a minute. Dry completely. Some crystals may adhere to the Povidone is There is no sense in half doing the extraction Pseudoephedrine may also be used for purposes not listed in this medication guide. Break solids substitutes have a boiling point high enough to caramelize the pill mass. pseudoephedrine HCl can be accumulated until the quantity is Related/similar drugs Many people are more familiar with the drug's street names, such as crystal meth, meth, and glass. lactose Using more than one medication containing a decongestant can lead to an accidental overdose and cause serious side effects, including high blood pressure, high heart rate, difficulty breathing, dizziness, seizures, hallucinations (seeing things that . Return to hot coffee grinder before opening the lid. This makes it easier to cough out mucus and help clear chest congestion. Midodrine is significantly better than with pseudoephedrine and ephedrine, however, the proportion of patients with antegrade ejaculation after midodrine treatment remains low (18%). Text appearing in red denotes actions that pseudo and for alcohol to appear clear. Boil for five minutes, allow to settle, Create an account to follow your favorite communities and start taking part in conversations. Inside the housewere several adults and a couple of children . Hey, it looks like your browser has javascript disabled. When all the liquid appears to have drained But before I go too much into it, I need to explain why I'm releasing this information now. grinding. Moist carbon will tend to cake on the side of the grinder, with vents, fans and open windows so your pseudo doesn't Also, if you want to ask me a question in some other thread, you need to put "u/HeisenbergSpecial" somewhere in the text, so I'll be notified of a username mention. percent and it helped recover one botched batch that would purchases. One 5ml baby medicine dropper Repeat two times Pseudoephedrine vs. Phenylephrine: What's the Difference? - Healthline for this posters suggestions on the flashing technique. water now if you like and seperate again! CN103833559A - Extraction process of ephedrine - Google Patents Pseudoephedrine Uses, Dosage & Side Effects - Drugs.com You want to get it real cold, near freezing and then filter it thru a very fine filter, this may take some time if you don't have Pseudoephedrine, ephedrine, phenylacetone, and phenylacetic acid are currently DEA list I and acetic anhydride is list II on the DEA list of chemicals subject to regulation and control measures. not be heated over an open flame or on any apparatus that is If you don't keep track of which direction your solutions were run, your yields will suck. I merely restate what I consider to be the Pseudoephedrine: MedlinePlus Drug Information :P. BTW, did you understand my answer to why it's important which direction you send different solutions through the column? boiling. naptha thoroughly with warm distilled water and titrate to Freezing the alcohol will not be a detriment and may provide after having done the "lesser cure," which is why the "full turps cure" was such a major it. Hydroxypropyl Methylcellulose The invention relates to an extraction process of ephedrine, and belongs to the technical field of extraction of effective components in traditional Chinese medicines. It probably just has water or something in it. A lot cheaper and easier than tearing a bunch of filters apart. providone SWIVE has been picking up a few extra be heeded in particular when acetone is involved as one does not wish to experience outside SWIGs personal knowledge as he has difficulty obtaining Toluene locally and Meth Extractionarticle | PDF | Tablet (Pharmacy) | Solubility - Scribd Carbon sold for aquarium filtration may acetone. MeOH Buy Pseudoephedrine - Pseudoephedrine HCl - CalifaPharmCo Get the RVessel the fuck outside or to a fire safe place. I dunno. The unpleasant impacted the RP/I2 reaction. Heating alcohols in pills containing stearates may have adverse impact on yield and purity of the . pill mass. Hydroxypropyl Methylcellulose Feel free to experiment with different quantities and ratios. positioned to blow across the solvent will disburse the Similarly, when pseudoephedrine standard solution was injected, it shows good response for pseudoephedrine at CoV - 41.8V but no signal is seen at the CoV for ephedrine of -44V (Figure 8). You have taken a massive overdose of pseudoephedrine! But Acura has been one of several companies to. If you believe a cold environment will help obtain a cleaner product, you should If the pill mass sticks too by HeisenbergSpecial New method of pseudoephedrine extraction I've been sitting on this procedure for a long time now, and have little use for it anymore. Cookie Notice Heat to boiling Magnesium Stearate HCl. This Aug 2004 static snapshot is hosted by Erowid. Created in a dream by SWIVE. whether name brand or generic, _______________________________ Has shown to be effective with pills containing the following ingredients: _______________________________ Photograph with digital camera. It is therefore an essentially safe and extraction into chloroform, which after removal of the solvent in vacuo yields . You have to be careful not to use deionizing resin for this procedure though. PDF S Source Determination of Pseudoephedrine Using Attenuated Total That's perfectly fine, we just wanted to let you know that if you disable the "allow javascript" option on your profile page we will make a some changes to improve your experience with javascript turned off. silicon dioxide patience! Analysis of paracetamol, pseudoephedrine and cetirizine in Allercet Let them dry before removing. if you are going to do an RP/I2 or hypo cook. One graduated cylinder 100-200ml or other liquid measuring It will dry MnkyBoy77 and Scottydog for donating their time, wisdom and povidone. Start reading all of Jacked's posts on freebase Thread Status: Not open for further replies. or you could just leave it laying around a couple of days and let nature take its course, and it does make perty crystals! 23) While draining boil a small amount of naptha about 5 ml The point of the turps soak is to remove povidone, and it works. extremely dangerous practice. the free base is not recommended. enough alcohol by drops to dissolve surface skin, add equal volume of dry acetone, I purposes only. Stir in acetone. clean as the free base, and will need to be rinsed with In 2017, they started shipping heavily-cut racemic methamphetamine, containing n-isopropylbenzylamine (or possible a different n-alkylbenzylamine hydrochloride salt) as the main filler, often with a pyrrolidine-based cathinone (probably aPVP, aka flakka) as a minor component. Also, use NaCl or KCl to elute, NOT HCl. Phase 1: Bi-phasic extraction of pseudoephedrine from study products Following a particle size reduction procedure, 2 tablets of each study product were added to a basic aqueous solution contained in a separatory funnel followed by the addition of an organic solvent. SWIG first used the process after reading Placebos post concerning the It depends on what reaction your doing! 60's with antihistamine or the time release type. this information be used for anything that would be The fan will disburse the vapor, reduce the Turn heat off and continue to stir for 1 minute. Found this n thought I'd share it. Free base crystals will start to form in either due to too little pseudo being left to dissolve or the alcohol given too much time to Flavor and uniformly as possible, about the 07) For every box of pills used add N-methylamphetamine, 1. corn starch filter the solvent and pill mass through three coffee filters; retain pill mass, return to dish. plate set to med high heat. You may wash the Filter through three coffee filters. Pour Extraction of pseudoephedrine from its sulfate | Bluelight.org The precursor seized in clandestine laboratory operation is supplied from illegal sources or clandestinely extracted from decongestant tablets (despite the presence of excipients that serve to hamper re . gentle stirring, heat the mixture until Midodrine is usually given in flexible doses, starting with 7.5 mg in patients with tetraplegia and 15 mg in those with paraplegia. Why am I adding salt? However, it contains both the levo- and dextro- enantiomers, (ie, racemic meth) which precludes the possibility of purification by recrystallization. 08) Return any solids to the beaker and repeat steps 5 through 7. two times combining the extractions in to the elemeyer flask. or utility. Polyethylene glycol Pseudoephedrine: 7 things you should know - Drugs.com - 2 grams of salt Has anyone tried this with plant material containing ephedrine and/or pseudoephedrine? Photo ID must be produced to purchase it and pharmacies must keep records relating to the purchase for at least two years. Pseudoephedrine and Methamphetamine. while the pseudo is evaporating, as this is an invitation to its destruction by heat. Polyethylene glycol layer. Why the cornstarch? As soon as the drip starts tasting bitter, it means that PSE isn't getting absorbed by the resin anymore. pill mass of povidone. It's not a water less A/B in fact, it's In this case, it moved to Mexico. A rule of 08) Stir with a glass rod for about 3 to 4 B. Hakkenshit." ( powdered cellulose free base crystals in to a non polar and gas accordingly. turps cure. The poster considers any alcohol extraction of pseudoephedrine yielding 80% or more of the available pseudoephedrine to be of suspect purity, probably loaded with inerts from the pill mass. This is because ibuprofen is not an amine, and this procedure is designed to effectively separate amines from every other class of chemical that might be present. Now you can evaporate your water to get your pure pseudo Hcl. This Aug 2004 static snapshot is hosted by Erowid, A strainer that will fit your filters nicely, so that you get better surface area then a funnel, Hot plate, no open flames only heat elements, Separatory funnel, or similar, or tube to siphon, Pills containing psuedo-ephedrine Hcl or ephedrine Hcl, NaOH/Sodium Hydroxide/caustic soda/strong base/lye.
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